ISO DIS 5725-2
Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
|Publication Date:||21 January 2019|
|ICS Code (Application of statistical methods):||03.120.30|
|ICS Code (Metrology and measurement in general):||17.020|
- amplifies the general principles to be observed in designing experiments for the numerical estimation of the precision of measurement methods by means of a collaborative interlaboratory experiment;
- provides a detailed practical description of the basic method for routine use in estimating the precision of measurement methods;
- provides guidance to all personnel concerned with designing, performing or analysing the results of the tests for estimating precision.
NOTE Modifications to this basic method for particular purposes are given in other parts of ISO 5725.
Annex C provides practical examples of estimating the precision of measurement methods by experiment.
This document is concerned exclusively with measurement methods which yield measurements on a continuous scale and give a single value as the test result, although this single value may be the outcome of a calculation from a set of observations.
It assumes that in the design and performance of the precision experiment, all the principles as laid down in ISO 5725-1 have been observed. The basic method uses the same number of test results in each laboratory, with each laboratory analysing the same levels of test sample; i.e. a balanced uniform-level experiment. The basic method applies to procedures that have been standardized and are in regular use in a number of laboratories.
NOTE Worked examples are given to demonstrate balanced uniform sets of test results, although in one example a variable number of replicates per cell were reported (unbalanced design) and in another some data were missing. This is because an experiment designed to be balanced can turn out to be unbalanced. Stragglers and outliers are also considered.
The statistical model of ISO 5725-1:1994,Clause 5, is accepted as a suitable basis for the interpretation and analysis of the test results, the distribution of which is approximately normal.
The basic method, as described in this document, will (usually) estimate the precision of a measurement method:
a) when it is required to determine the repeatability and reproducibility standard deviations as defined in ISO 5725-1;
b) when the materials to be used are homogeneous, or when the effects of heterogeneity can be included in the precision values; and
c) when the use of a balanced uniform-level layout is acceptable.