UNLIMITED FREE ACCESS TO THE WORLD'S BEST IDEAS

SUBMIT
Already a GlobalSpec user? Log in.

This is embarrasing...

An error occurred while processing the form. Please try again in a few minutes.

Customize Your GlobalSpec Experience

Finish!
Privacy Policy

This is embarrasing...

An error occurred while processing the form. Please try again in a few minutes.

D4274

Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols

inactive
Publication Date: 1 July 2021
Status: inactive
Page Count: 10
ICS Code (Thermoplastic materials): 83.080.20
scope:

These test methods measure the hydroxyl groups in polyester and polyether polyols containing primary and secondary hydroxyl groups. They also apply to many other hydroxyl-containing substances.

Test Method A-Acetic Anhydride Pressure Bottle, recommended for polyesters.

Test Method B-Phthalic Anhydride Pressure Bottle, recommended for polyethers and polyesters.

Test Method C-Phthalic Anhydride Reflux, recommended for polyethers and polyesters.

Test Method D-Imidazole-Catalyzed Phthalic Anhydride Pressure Bottle, recommended for polyethers, polyesters, polymer polyols, and amine-initiated polyols.

Test Method E-Imidazole-Catalyzed Pyromellitic Dianhydride Esterification, recommended for polyols used for flexible and rigid polyurethane foams and urethane elastomers. It is recommended for polyester polyols, polyether polyols, amine-started polyols, and polymer polyols (polyacrylonitrile/copolystyrene-based).

Another ASTM test method for measuring hydroxyl groups is Test Method E222.

The values stated in SI units are to be regarded as the standard.

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

NOTE 1-This standard, ISO 14900 and ISO 6796 address the same subject matter, but differ in technical content.

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

*A Summary of Changes section appears at the end of this standard

Document History

March 15, 2023
Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
These test methods measure the hydroxyl groups in polyester and polyether polyols containing primary and secondary hydroxyl groups. They also apply to many other hydroxyl-containing substances. Test...
D4274
July 1, 2021
Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
These test methods measure the hydroxyl groups in polyester and polyether polyols containing primary and secondary hydroxyl groups. They also apply to many other hydroxyl-containing substances. Test...
April 1, 2016
Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
These test methods measure the hydroxyl groups in polyester and polyether polyols containing primary and secondary hydroxyl groups. They also apply to many other hydroxyl-containing substances. Test...
February 1, 2011
Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
These test methods measure the hydroxyl groups in polyester and polyether polyols containing primary and secondary hydroxyl groups. They also apply to many other hydroxyl-containing substances. ...
July 1, 2005
Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
(Footnote *) These test methods measure the hydroxyl groups in polyester and polyether polyols containing primary and secondary hydroxyl groups. They also apply to many other hydroxyl-containing...
November 10, 1999
Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
These test methods measure the hydroxyl groups in polyester and polyether polyols containing primary and secondary hydroxyl groups. They also apply to many other hydroxyl-containing substances. Test...
October 15, 1994
Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
A description is not available for this item.
November 25, 1988
STANDARD TEST METHODS FOR TESTING POLYURETHANE RAW MATERIALS: DETERMINATION OF HYDROXYL NUMBERS OF POLYOLS (E1-1990) (E2-1992)
A description is not available for this item.
July 29, 1983
STANDARD METHOD FOR TESTING POLYURETHANE POLYOL RAW MATERIALS: DETERMINATION OF HYDROXYL NUMBERS OF POLYOLS
A description is not available for this item.

References

Advertisement