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ASTM D2892

Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)

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Organization: ASTM
Publication Date: 1 July 2017
Status: inactive
Page Count: 34
ICS Code (Crude petroleum): 75.040
scope:

This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400 °C Atmospheric Equivalent Temperature (AET). This test method employs a fractionating column having an efficiency of 14 to 18 theoretical plates operated at a reflux ratio of 5:1. Performance criteria for the necessary equipment is specified. Some typical examples of acceptable apparatus are presented in schematic form. This test method offers a compromise between efficiency and time in order to facilitate the comparison of distillation data between laboratories.

NOTE 1-Defined as having a Reid vapor pressure less than 82.7 kPa (12 psi).

This test method details procedures for the production of a liquefied gas, distillate fractions, and residuum of standardized quality on which analytical data can be obtained, and the determination of yields of the above fractions by both mass and volume. From the preceding information, a graph of temperature versus mass % distilled can be produced. This distillation curve corresponds to a laboratory technique, which is defined at 15/5 (15 theoretical plate column, 5:1 reflux ratio) or TBP (true boiling point).

This test method can also be applied to any petroleum mixture except liquefied petroleum gases, very light naphthas, and fractions having initial boiling points above 400 °C.

This test method contains the following annexes and appendixes:

Annex A1-Test Method for the Determination of the Efficiency of a Distillation Column,

Annex A2-Test Method for the Determination of the Dynamic Holdup of a Distillation Column,

Annex A3-Test Method for the Determination of the Heat Loss in a Distillation Column (Static Conditions),

Annex A4-Test Method for the Verification of Temperature Sensor Location,

Annex A5-Test Method for Determination of the Temperature Response Time,

Annex A6-Practice for the Calibration of Sensors,

Annex A7-Test Method for the Verification of Reflux Dividing Valves,

Annex A8-Practice for Conversion of Observed Vapor Temperature to Atmospheric Equivalent Temperature (AET),

Appendix X1-Test Method for Dehydration of a Sample of Wet Crude Oil, and

Appendix X2-Practice for Performance Check.

The values stated in SI units are to be regarded as the standard.

Exception-The values given in parentheses are for information only.

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 10.

WARNING-Mercury has been designated by many regulatory agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA's website-http://www.epa.gov/mercury/faq.htm-for additional information. Users should be aware that selling mercury and/or mercury containing products into your state or country may be prohibited by law.

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

*A Summary of Changes section appears at the end of this standard

Document History

June 1, 2020
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400 °C Atmospheric Equivalent Temperature (AET). This test method...
November 1, 2019
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400 °C Atmospheric Equivalent Temperature (AET). This test method...
December 1, 2018
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400 °C Atmospheric Equivalent Temperature (AET). This test method...
April 1, 2018
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400 °C Atmospheric Equivalent Temperature (AET). This test method...
ASTM D2892
July 1, 2017
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400 °C Atmospheric Equivalent Temperature (AET). This test method...
May 1, 2017
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400 °C Atmospheric Equivalent Temperature (AET). This test method...
December 1, 2016
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400 °C Atmospheric Equivalent Temperature (AET). This test method...
April 1, 2015
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400 °C Atmospheric Equivalent Temperature (AET). This test method...
May 1, 2013
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400°C Atmospheric Equivalent Temperature (AET). This test method...
December 1, 2011
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum to a final cut temperature of 400°C Atmospheric Equivalent Temperature (AET). This test method employs a...
July 1, 2011
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400°C Atmospheric Equivalent Temperature (AET). This test method...
October 1, 2010
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400°C Atmospheric Equivalent Temperature (AET). This test method...
November 1, 2005
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
*  This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400°C Atmospheric Equivalent Temperature (AET). This test method...
November 1, 2003
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
A description is not available for this item.
June 10, 2003
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum (See Note 1) to a final cut temperature of 400°C Atmospheric Equivalent Temperature (AET). This test method...
December 10, 2001
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
This test method covers the procedure for the distillation of stabilized crude petroleum to a final cut temperature of 400°C Atmospheric Equivalent Temperature (AET). This test method employs a...
November 10, 1999
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
Scope This test method covers the procedure for the distillation of stabilized crude petroleum to a final cut temperature of 400°C AET (Atmospheric Equivalent Temperature). The test method employs a...
April 10, 1999
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
A description is not available for this item.
November 10, 1998
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
A description is not available for this item.
June 10, 1998
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
A description is not available for this item.
January 1, 1995
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
A description is not available for this item.
December 27, 1990
STANDARD TEST METHOD FOR DISTILLATION OF CRUDE PETROLEUM (15-THEORETICAL PLATE COLUMN) (E1-1991)
A description is not available for this item.
June 29, 1984
STANDARD TEST METHOD FOR DISTILLATION OF CRUDE PETROLEUM (15- THEORETICAL PLATE COLUMN)
A description is not available for this item.

References

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