ASTM E299

Standard Test Method for Trace Amounts of Peroxides In Organic Solvents

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Organization: ASTM
Publication Date: 1 July 2017
Status: active
Page Count: 4
ICS Code (Other products of the chemical industry): 71.100.99
scope:

This test method2,3 covers organic solvents containing active oxygen in the range from 5 to 80 μg/g (ppm) or higher. By using a special reaction-absorption cell, the test method can be extended to cover the range from 0 to 5 ppm. The test method can be used to determine numerous peroxide classes of varying reactivity such as hydroperoxides, diacyl peroxides, diaroyl peroxides, peresters, and ketone peroxides. The stable di-tert-alkyl peroxides do not react under the conditions of analysis.

Solvents that can be analyzed successfully include saturated and aromatic hydrocarbons, alcohols, ethers, ketones, and esters. In addition, the test method is applicable to olefinic solvents and to certain compounds that contain α, β, and conjugated unsaturation. Solid samples that are soluble in the acetic acid-chloroform solvent also can be analyzed.

Review the current Safety Data Sheets (SDS) for detailed information concerning toxicity, first aid practices, and safety precautions.

The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.

This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

2 Banerjee, D. K., and Budke, C. C., Analytical Chemistry, ANCHAM, Vol 36, 1964, pp. 792-796.

3 Banerjee, D. K., and Budke, C. C., Analytical Chemistry, ANCHAM, Vol 36, 1964, pp. 2367-2368.

*A Summary of Changes section appears at the end of this standard

Document History

ASTM E299
July 1, 2017
Standard Test Method for Trace Amounts of Peroxides In Organic Solvents
This test method2,3 covers organic solvents containing active oxygen in the range from 5 to 80 μg/g (ppm) or higher. By using a special reaction-absorption cell, the test method can be extended to...
February 1, 2017
Standard Test Method for Trace Amounts of Peroxides In Organic Solvents
This test method2,3 covers organic solvents containing active oxygen in the range from 5 to 80 μg/g (ppm) or higher. By using a special reaction-absorption cell, the test method can be extended to...
April 1, 2008
Standard Test Method for Trace Amounts of Peroxides In Organic Solvents
This test method2,3 covers organic solvents containing active oxygen in the range from 5 to 80 µg/g (ppm) or higher. By using a special reaction-absorption cell, the test method can be extended to...
July 10, 1997
Standard Test Method for Trace Amounts of Peroxides in Organic Solvents
This test method covers organic solvents containing active oxygen in the range from 5 to 80 ppm or higher. By using a special reaction-absorption cell, the test method can be extended to cover the...
July 10, 1997
Standard Test Method for Trace Amounts of Peroxides in Organic Solvents
1. Scope 1.1 This test method covers organic solvents containing active oxygen in the range from 5 to 80 ppm or higher. By using a special reaction-absorption cell, the test method can be extended to...
January 1, 1990
Standard Test Method for Trace Amounts of Peroxides in Organic Solvents
A description is not available for this item.
August 25, 1989
STANDARD TEST METHOD FOR TRACE AMOUNTS OF PEROXIDES IN ORGANIC SOLVENTS
A description is not available for this item.
July 27, 1984
STANDARD TEST METHOD FOR TRACE AMOUNTS OF PEROXIDES IN ORGANIC SOLVENTS
A description is not available for this item.

References

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