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ASTM International - ASTM D4929-17

Standard Test Method for Determination of Organic Chloride Content in Crude Oil

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Organization: ASTM International
Publication Date: 15 October 2017
Status: inactive
Page Count: 17
ICS Code (Crude petroleum): 75.040
significance And Use:

4.1 Organic chlorides do not occur naturally in crude oil. When present, they result from contamination in some manner, such as disposal of chlorinated solvent used in many dewaxing pipeline or... View More

scope:

1.1 The procedures in this test method cover the determination of organic chloride (above 1 μg/g organically-bound chlorine) in crude oils, using either distillation and sodium biphenyl reduction, distillation and microcoulometry, or distillation and x-ray fluorescence (XRF) spectrometry.

1.2 The procedures in this test method involve the distillation of crude oil test specimens to obtain a naphtha fraction prior to chloride determination. The chloride content of the naphtha fraction of the whole crude oil can thereby be obtained. See Section 5 regarding potential interferences.

1.3 Procedure A covers the determination of organic chloride in the washed naphtha fraction of crude oil by sodium biphenyl reduction followed by potentiometric titration.

1.4 Procedure B covers the determination of organic chloride in the washed naphtha fraction of crude oil by oxidative combustion followed by microcoulometric titration.

1.5 Procedure C covers the determination of organic chloride in the washed naphtha fraction of crude oil by x-ray fluorescence spectrometry.

1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6.1 The preferred concentration units are micrograms of chloride per gram of sample.

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Document History

October 1, 2022
Standard Test Method for Determination of Organic Chloride Content in Crude Oil
1.1 The procedures in this test method cover the determination of organic chloride (above 1 μg/g organically-bound chlorine) in crude oils, using either distillation and sodium biphenyl reduction,...
December 1, 2019
Standard Test Method for Determination of Organic Chloride Content in Crude Oil
1.1 The procedures in this test method cover the determination of organic chloride (above 1 μg/g organically-bound chlorine) in crude oils, using either distillation and sodium biphenyl reduction,...
July 1, 2019
Standard Test Method for Determination of Organic Chloride Content in Crude Oil
1.1 The procedures in this test method cover the determination of organic chloride (above 1 μg/g organically-bound chlorine) in crude oils, using either distillation and sodium biphenyl reduction,...
ASTM D4929-17
October 15, 2017
Standard Test Method for Determination of Organic Chloride Content in Crude Oil
4.1 Organic chlorides do not occur naturally in crude oil. When present, they result from contamination in some manner, such as disposal of chlorinated solvent used in many dewaxing pipeline or other...
October 1, 2016
Standard Test Method for Determination of Organic Chloride Content in Crude Oil
4.1 Organic chlorides do not occur naturally in crude oil. When present, they result from contamination in some manner, such as disposal of chlorinated solvent used in many dewaxing pipeline or other...
December 1, 2015
Standard Test Methods for Determination of Organic Chloride Content in Crude Oil
4.1 Organic chlorides do not occur naturally in crude oil. When present, they result from contamination in some manner, such as disposal of chlorinated solvent used in many dewaxing pipeline or other...
June 1, 2015
Standard Test Methods for Determination of Organic Chloride Content in Crude Oil
4.1 Usually organic chlorides do not occur naturally in crude oil. When present, they result from contamination in some manner, such as disposal of waste solvent or as use for dewaxing a pipeline or...
May 1, 2014
Standard Test Methods for Determination of Organic Chloride Content in Crude Oil
1.1 These test methods cover the determination of organic chloride (above 1 μg/g organically-bound chlorine) in crude oils, using either distillation and sodium biphenyl reduction or distillation and...
November 1, 2007
Standard Test Methods for Determination of Organic Chloride Content in Crude Oil
1.1 These test methods cover the determination of organic chloride (above 1 μg/g organically-bound chlorine) in crude oils, using either distillation and sodium biphenyl reduction or distillation and...
November 1, 2004
Standard Test Methods for Determination of Organic Chloride Content in Crude Oil
1.1 These test methods cover the determination of organic chloride (above 1 g/g organically-bound chlorine) in crude oils, using either distillation and sodium biphenyl reduction or distillation and...
January 10, 1999
Standard Test Methods for Determination of Organic Chloride Content in Crude Oil
1.1 These test methods cover the determination of organic chloride (above 1 g/g organically-bound chlorine) in crude oils, using either distillation and sodium biphenyl reduction or distillation and...
January 10, 1999
Standard Test Methods for Determination of Organic Chloride Content in Crude Oil
1.1 These test methods cover the determination of organic chloride (above 1 [mu]g/g organically-bound chlorine) in crude oils, using either distillation and sodium biphenyl reduction or distillation...
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