NEN-EN 16159
Animal feeding stuffs - Determination of selenium by hydride generation atomic absorption spectrometry (HGAAS) after microwave digestion (extraction with 65% nitric acid and 30% hydrogen peroxide)
| Organization: | NEN |
| Publication Date: | 1 October 2010 |
| Status: | inactive |
| Page Count: | 19 |
| ICS Code (Animal feeding stuffs): | 65.120 |
scope:
This European Standard specifies a method for the determination of selenium in animal feeding stuffs by hydride generation atomic absorption spectrometry (HGAAS) after microwave pressure digestion. The method was successfully tested by an inter-laboratory study of CEN/TC 327/WG 4 in the range of 0,25 mg/kg to 74 mg/kg. The limit of quantification is 0,5 μg/l of the test solution which corresponds to the calibration standard 2. Using a test portion of 0,5 g and a volume of the test solution of 25 ml after pressure digestion the limit of quantification is calculated as 0,125 mg/kg in the feed material.
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