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NEN - NVN-ENV 14194

Foodstuffs - Determination of saxitoxin and dc- saxitoxin in mussels - HPLC method using post column derivatisation

active, Most Current
Organization: NEN
Publication Date: 1 May 2002
Status: active
Page Count: 17
ICS Code (Fish and fishery products): 67.120.30
scope:

Specifies a method for the quantitative determination of saxitoxin (STX), dc-saxitoxin (dc-STX) and the qualitative determination of neo-saxitoxin, and the gonyautoxins GTX-2 and GTX-3 in mussels. The method can also be used to identify the N-sulfocarbamoyl toxins C-1, C-2, GTX-5 and GTX-6 after hydrolysis and, if these toxins are present, to exclude false positive results for GTX-2, GTX-3, neo-saxitoxin and saxitoxin. For mussel the limit of quantification is for saxitoxin 0,04 mg/kg mussel meat and for dc-saxitoxin 0,03 mg/kg mussel meat (signal/noise = 10).

Document History

NVN-ENV 14194
May 1, 2002
Foodstuffs - Determination of saxitoxin and dc- saxitoxin in mussels - HPLC method using post column derivatisation
Specifies a method for the quantitative determination of saxitoxin (STX), dc-saxitoxin (dc-STX) and the qualitative determination of neo-saxitoxin, and the gonyautoxins GTX-2 and GTX-3 in mussels....
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