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ASTM D664

Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration

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Organization: ASTM
Publication Date: 1 November 2018
Status: active
Page Count: 11
ICS Code (Petroleum products in general): 75.080
scope:

This test method covers procedures for the determination of acidic constituents in petroleum products, lubricants, biodiesel, and blends of biodiesel.

Test Method A-For petroleum products and lubricants soluble or nearly soluble in mixtures of toluene and propan-2- ol. It is applicable for the determination of acids whose dissociation constants in water are larger than 10-9; extremely weak acids whose dissociation constants are smaller than 10-9 do not interfere. Salts react if their hydrolysis constants are larger than 10-9. The range of acid numbers included in the precision statement is 0.1 mg ⁄g KOH to 150 mg ⁄g KOH.

Test Method B-Developed specifically for biodiesel and biodiesel blends with low acidity and slightly different solubility. This test method requires the use of an automatic titrator with automatic endpoint-seeking capability.

NOTE 1-In new and used oils, the constituents that may be considered to have acidic characteristics include organic and inorganic acids, esters, phenolic compounds, lactones, resins, salts of heavy metals, salts of ammonia and other weak bases, acid salts of polybasic acids, and addition agents such as inhibitors and detergents.

The test method may be used to indicate relative changes that occur in oil during use under oxidizing conditions regardless of the color or other properties of the resulting oil. Although the titration is made under definite equilibrium conditions, the test method is not intended to measure an absolute acidic property that can be used to predict performance of oil under service conditions. No general relationship between bearing corrosion and acid number is known.

NOTE 2-The acid number obtained by this standard may or may not be numerically the same as that obtained in accordance with Test Methods D974 and D3339. There has not been any attempt to correlate this method with other non-titration methods.

NOTE 3-A few laboratories have made the observation that there is a difference in Test Method D664 results when aqueous versus nonaqueous buffers are used.

The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

* A Summary of Changes section appears at the end of this standard

Document History

ASTM D664
November 1, 2018
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products, lubricants, biodiesel, and blends of biodiesel. Test Method A—For petroleum products and...
November 1, 2018
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products, lubricants, biodiesel, and blends of biodiesel. Test Method A—For petroleum products and...
November 1, 2018
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products, lubricants, biodiesel, and blends of biodiesel. Test Method A—For petroleum products and...
December 15, 2017
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products, lubricants, biodiesel, and blends of biodiesel. Test Method A—For petroleum products and...
October 1, 2017
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products, lubricants, biodiesel, and blends of biodiesel. Test Method A—For petroleum products and...
July 15, 2011
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products, lubricants, biodiesel and blends of biodiesel. Test Method A—For petroleum products and...
July 15, 2011
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products, lubricants, biodiesel and blends of biodiesel. Test Method A—For petroleum products and...
July 15, 2011
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products, lubricants, biodiesel and blends of biodiesel. Test Method A—For petroleum products and...
May 15, 2011
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products, lubricants, biodiesel and blends of biodiesel. Test Method A—For petroleum products and...
December 15, 2009
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products, lubricants, biodiesel and blends of biodiesel. Test Method A—For petroleum products and...
March 1, 2009
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products, lubricants, biodiesel and blends of biodiesel. Test Method A—For petroleum products and...
July 1, 2007
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products and lubricants soluble or nearly soluble in mixtures of toluene and propan-2-ol. It is applicable...
November 1, 2006
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products and lubricants soluble or nearly soluble in mixtures of toluene and propan-2-ol. It is applicable...
November 1, 2006
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products and lubricants soluble or nearly soluble in mixtures of toluene and propan-2- ol. It is...
January 1, 2006
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products and lubricants soluble or nearly soluble in mixtures of toluene and propan-2- ol. It is...
February 1, 2004
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
(Footnote *) This test method covers procedures for the determination of acidic constituents in petroleum products and lubricants soluble or nearly soluble in mixtures of toluene and propan-2-ol. It...
February 1, 2004
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
(Footnote *) This test method covers procedures for the determination of acidic constituents in petroleum products and lubricants soluble or nearly soluble in mixtures of toluene and propan-2-ol. It...
November 10, 2001
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
This test method covers procedures for the determination of acidic constituents in petroleum products and lubricants soluble or nearly soluble in mixtures of toluene and propan-2-ol (Note 1). It is...
October 10, 1995
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
1. Scope 1.1 This test method covers procedures for the determination of acidic constituents in petroleum products and lubricants soluble or nearly soluble in mixtures of toluene and propan-2-ol...
January 1, 1995
Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
1. Scope 1.1 This test method covers procedures for the determination of acidic constituents in petroleum products and lubricants soluble or nearly soluble in mixtures of toluene and propan-2-ol...
December 21, 1989
STANDARD TEST METHOD FOR ACID NUMBER OF PETROLEUM PRODUCTS BY POTENTIOMETRIC TITRATION (BRITISH STANDARD 4457) (IP DESIGNATION: 177/83)
A description is not available for this item.
October 30, 1987
STANDARD TEST METHOD FOR ACID NUMBER OF PETROLEUM PRODUCTS BY POTENTIOMETRIC TITRATION (BRITISH STANDARD 4457) (IP 177/83)
A description is not available for this item.
August 28, 1981
STANDARD TEST METHOD FOR NEUTRALIZATION NUMBER BY POTENTIOMETRIC TITRATION
A description is not available for this item.

References

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