DIN SPEC 91127
Recommendation for Temperature Calibration of Fast Scanning Calorimeters (FSCs) for Sample Mass and Scan Rate; Text in English
|Publication Date:||1 June 2011|
|ICS Code (Heat. Calorimetry):||17.200.10|
This specification describes a protocol of temperature calibration procedures for Fast Scanning Calorimeters for high to very high scan rates and low to very low sample masses, respectively, thus complementing ISO 11357.
Procedures are given for both an extensive temperature calibration as well as a rather quick temperature calibration of FSCs in the heating and the cooling modes for various scan rates and concomitant adjusted sample masses.
Thus, the specification also facilitates making the right choices to minimize the thermal lag arising at increasing scan rates before performing a measurement.