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CEN - EN 17250

Foodstuffs - Determination of ochratoxin A in spices, liquorice, cocoa and cocoa products by IAC clean-up and HPLC-FLD

active, Most Current
Organization: CEN
Publication Date: 1 January 2020
Status: active
Page Count: 30
ICS Code (Spices and condiments): 67.220.10
ICS Code (Cocoa): 67.140.30
scope:

This document specifies a procedure for the determination of ochratoxin A (OTA) in chilli, paprika, black and white pepper, nutmeg, spice mix, liquorice (root and extracts), cocoa and cocoa products by high performance liquid chromatography (HPLC) with immunoaffinity column clean-up and fluorescence detection (FLD).

This method has been validated in interlaboratory studies via the analysis of both naturally contaminated and spiked samples ranging from 1,0 μg/kg to 84,9 μg/kg for spices (paprika and chili [5], black and white pepper, nutmeg and spice mix [6]), ranging from 7,7 μg/kg to 96,8 μg/kg for liquorice and liquorice products [7] and ranging from 2,1 μg/kg to 26,3 μg/kg for cocoa and cocoa products [6].

For further information on the validation, see Clause 10 and Annex B.

 

 

Document History

EN 17250
January 1, 2020
Foodstuffs - Determination of ochratoxin A in spices, liquorice, cocoa and cocoa products by IAC clean-up and HPLC-FLD
This document specifies a procedure for the determination of ochratoxin A (OTA) in chilli, paprika, black and white pepper, nutmeg, spice mix, liquorice (root and extracts), cocoa and cocoa products...

References

This document references:
EN ISO 3696 - Water for Analytical Laboratory Use- Specification and Test Methods
Published by CEN on January 1, 1995
A description is not available for this item.
This document references:
EN ISO/IEC 17025 - General requirements for the competence of testing and calibration laboratories
Published by CEN on December 1, 2017
This document specifies the general requirements for the competence, impartiality and consistent operation of laboratories. This document is applicable to all organizations performing laboratory...
This document references:
NO 1907/2006 CORR - CORRIGENDA Corrigendum to Regulation the European Parliament and of the Council of 18 December 2006 concerning the Registration, Evaluation, Authorisation and Restriction of Chemicals (REACH), establishing a European Chemicals Agency, amending Directive 1999/45/EC and repealing Council Regulation (EEC) No 793/93 and Commission Regulation (EC) No 1488/94 as well as Council Directive 76/769/EEC and Commission Directives 91/155/EEC, 93/67/EEC, 93/105/EC and 2000/21/EC
Published by EU on May 31, 2008
A description is not available for this item.
This document references:
5725-1 - Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
Published by ISO on July 1, 2023
This document — introduces conditions, constraints and resources necessary to evaluate a measurement method or a result; — defines an organizational scheme for the acquisition of trueness and...
This document references:
ISO 5725-2 - Accuracy (trueness and precision) of measurement methods and results — Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
Published by ISO on December 1, 2019
This document — amplifies the general principles for designing experiments for the numerical estimation of the precision of measurement methods by means of a collaborative interlaboratory experiment;...
This document references:
ISO 5725-3 - Accuracy (Trueness and Precision) of Measurement Methods and Results - Part 3: Intermediate Measures of the Precision of a Standard Measurement Method
Published by ISO on January 1, 1994
A description is not available for this item.
This document references:
ISO 5725-4 - Accuracy (trueness and precision) of measurement methods and results — Part 4: Basic methods for the determination of the trueness of a standard measurement method
Published by ISO on March 1, 2020
This document — specifies basic methods for estimating the bias of a measurement method and the laboratory bias when a measurement method is applied; — provides a practical approach of a basic method...
This document references:
ISO 5725-5 - Accuracy (Trueness and Precision) of Measurement Methods and Results - Part 5: Alternative Methods for the Determination of the Precision of a Standard Measurement Method
Published by ISO on July 15, 1998
A description is not available for this item.
This document references:
ISO 5725-6 - Accuracy (Trueness and Precision) of Measurement Methods and Results - Part 6: Use in Practice of Accuracy Values
Published by ISO on January 1, 1994
A description is not available for this item.
This document references:
ISO/IEC 17025 - General requirements for the competence of testing and calibration laboratories
Published by ISO on November 1, 2017
This document specifies the general requirements for the competence, impartiality and consistent operation of laboratories. This document is applicable to all organizations performing laboratory...
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