Standard Practice for Measuring and Scoring Performance of Trace Explosive Chemical Detectors
|Publication Date:||1 February 2021|
|ICS Code (Explosion protection):||13.230|
This practice may be used for measuring, scoring, and improving the overall performance of detectors that alarm on traces of explosives on swabs. These explosive trace detectors (ETDs) may be based on, but are not limited to, chemical detection technologies such as ion mobility spectrometry (IMS) and mass spectrometry (MS).
This practice considers instrumental (post-sampling) trace detection performance, involving specific chemical analytes across eight types of explosive formulations in the presence of a standard background challenge material. This practice adapts Test Method E2677 for the evaluation of limit of detection, a combined metric of measurement sensitivity and repeatability, which requires ETDs to have numerical responses.
This practice considers the effective detection throughput of an ETD by factoring in the sampling rate, interrogated swab area, and estimated maintenance requirements during a typical eight hour shift.
This practice does not require, but places extra value on, the specific identification of targeted compounds and explosive formulations.
The functionality of multi-mode instruments (those that may be switched between detection of trace explosives, drugs of interest, chemical warfare agents, and other target compounds) may also be tested. A multi-mode instrument under test shall be set to the mode that optimizes operational conditions for the detection of trace explosives. This practice requires the use of a single set of ETD operational settings for calculating a system test score based on the factors described in 1.2, 1.3, and 1.4. A minimum acceptable score is derived from criteria established in Practice E2520 - 07, and an example of such a test is presented in Appendix X1 (Example 2).
Intended Users-ETD developers and manufacturers, testing laboratories, and international agencies responsible for enabling effective deterrents to terrorism.
Actual explosives as test samples would be preferable, but standard explosive formulations are not widely available, nor are methods for depositing these quantitatively and realistically on swabs. This practice considers sixteen compounds that are available from commercial suppliers. This does not imply that only these sixteen are important to trace detection. Most ETDs are able to detect many other compounds, but these are either chemically similar (hence redundant) to the ones considered, or are unavailable from commercial suppliers for reasons of stability and safety. Under typical laboratory practices, the sixteen compounds considered are safe to handle in the quantities used.
This practice is not intended to replace any current standard procedure employed by agencies to test performance of ETDs for specific applications. Those procedures may be more rigorous, use different compounds or actual explosive formulations, employ different or more realistic background challenges, and consider environmental sampling procedures and other operational variables.
This practice recommends one method for preparation of test swabs, pipetting, because this method is simple, reproducible, quantitative, documented, and applicable to most current detection technologies. Other methods, such as inkjet printing and dry transfer, may generate more realistic analyte distributions and particle sizes, but these methods are not widely available and less familiar. They may be used if the procedures are validated and documented properly.
With any deposition method, some compounds are difficult to present to the ETD inlet quantitatively due to volatility and loss during the swab preparation process. Problematic issues pertinent to this practice are identified along with recommended instructions.
Units-The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.