DS/ISO 18363-3
Animal and vegetable fats and oils – Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS – Part 3: Method using acid transesterification and measurement for 2-MCPD, 3-MCPD and glycidol
active, Most Current
| Organization: | DS |
| Publication Date: | 15 June 2021 |
| Status: | active |
| Page Count: | 28 |
| ICS Code (Animal and vegetable fats and oils): | 67.200.10 |
scope:
ISO 18363-3:2017 specifies a procedure for the simultaneous determination of 2-MCPD esters (bound 2-MCPD), 3‐MCPD esters (bound 3‐MCPD) and glycidyl esters (bound glycidol) in a single assay, based on acid catalysed ester cleavage and derivatization of cleaved (free) analytes with phenylboronic acid (PBA) prior to GC/MS analysis. ISO 18363-3:2017 is applicable to solid and liquid fats and oils. For all three analytes the limit of quantification (LOQ) is 0,1 mg/kg and the limit of detection (LOD) is 0,03 mg/kg.
Document History
DS/ISO 18363-3
June 15, 2021
Animal and vegetable fats and oils – Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS – Part 3: Method using acid transesterification and measurement for 2-MCPD, 3-MCPD and glycidol
ISO 18363-3:2017 specifies a procedure for the simultaneous determination of 2-MCPD esters (bound 2-MCPD), 3‐MCPD esters (bound 3‐MCPD) and glycidyl esters (bound glycidol) in a single...