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ASTM International - ASTM E2941-21

Standard Practices for Extraction of Elements from Ores and Related Metallurgical Materials by Acid Digestion

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Organization: ASTM International
Publication Date: 1 October 2021
Status: active
Page Count: 5
ICS Code (Metalliferous minerals in general): 73.060.01
significance And Use:

4.1 These practices are primarily intended to test materials for compliance with compositional specifications and for monitoring. Partial extraction of ores and related metallurgical materials can... View More

scope:

1.1 These practices cover the digestion of ores and related metallurgical materials, such as mine soil, waste rock and tailings, for subsequent determination of acid-extractable contents of certain elements by such solution analytical techniques as atomic absorption spectrometry (AAS), inductively coupled plasma atomic emission spectrometry (ICP-AES) (see Test Method D1976), and inductively coupled plasma mass spectrometry (ICP-MS) (see Test Method D5673).

1.1.1 Contents of aluminum, antimony, arsenic, barium, beryllium, bismuth, boron, cadmium, calcium, chromium, cobalt, copper, gallium, iron, lead, lithium, magnesium, manganese, mercury, molybdenum, nickel, phosphorus, potassium, scandium, selenium, silver, sodium, strontium, thallium, tin, titanium, vanadium and zinc can be extracted from ores and related metallurgical materials for determination by analytical methods for elements in solution. Other elements may be determined from extracts produced using this practice.

1.1.2 Actual element quantification in digested solutions can be accomplished by following the various test methods under other appropriate ASTM standards for element(s) of interest in solution.

1.1.3 The detection limit and linear content range for each element is dependent on the atomic absorption, mass spectrometry or emission spectrometric technique employed and may be found in the manual accompanying the instrument used or ASTM standard method for analysis of the solutions. Consider the dilution factor in content calculations due to digestion and dilution of solid samples.

1.1.4 The extent of extraction of elements from ores and related metallurgical materials by these practices is dependent upon the physical and mineralogical characteristics of the prepared sample and the digestion practice used.

1.2 The digestion practices appear in the following order:

Sections
Nitric Acid Microwave Digestion 7 to 14
Four-Acid Total Digestion 15 to 21

1.3 The values stated SI units are to be regarded as the standard. No other units of measurements are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 11 and 20.

1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Document History

ASTM E2941-21
October 1, 2021
Standard Practices for Extraction of Elements from Ores and Related Metallurgical Materials by Acid Digestion
1.1 These practices cover the digestion of ores and related metallurgical materials, such as mine soil, waste rock and tailings, for subsequent determination of acid-extractable contents of certain...
November 1, 2014
Standard Practices for Extraction of Elements from Ores and Related Metallurgical Materials by Acid Digestion
1.1 These practices cover the digestion of ores and related metallurgical materials, such as mine soil, waste rock and tailings, for subsequent determination of acid-extractable contents of certain...
October 1, 2013
Standard Practice for Nitric Acid-Extraction of Elements from Ores and Related Metallurgical Materials by Closed Vessel Microwave Heating
1.1 This practice covers the digestion of ores and related metallurgical materials, such as mine soil, waste rock and tailings, for subsequent determination of nitric acid-extractable contents of...
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