IEC - 62321-11
Determination of certain substances in electrotechnical products – Part 11: Tris(2-chloroethyl) phosphate (TCEP) in plastics by gas chromatography-mass spectrometry (GC-MS) and liquid chromatography-mass spectrometry (LC-MS)
| Organization: | IEC |
| Publication Date: | 1 December 2023 |
| Status: | active |
| Page Count: | 78 |
| ICS Code (Environment and environmental protection in general): | 13.020.01 |
| ICS Code (Electrical and electronic equipment): | 43.040.10 |
scope:
This part of IEC 62321 specifies two different techniques for the determination of tris(2-chloroethyl) phosphate (TCEP) in plastics, the GC-MS or LC-MS method, both of which are applicable to quantitative analysis.
These two techniques are applicable to use with polyurethane, polyvinylchloride, and polyethylene materials containing TCEP between 200 mg/kg to 2 000 mg/kg.
These test methods do not apply to plastic materials having a processing temperature higher than 230 °C.
GC-MS using a pyrolyser/thermal desorption accessory (Py/TD-GC-MS) technique is described in Annex A and can be used for the screening of TCEP in plastics.
NOTE TCEP starts thermal decomposition at approximately 230 °C. Polymer types that have a processing temperature into shapes of plastics (e.g. pellets, moulded parts or sheets) not exceeding the decomposition temperature can contain TCEP.
Document History
