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ASTM International - ASTM D5198-09

Standard Practice for Nitric Acid Digestion of Solid Waste

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Organization: ASTM International
Publication Date: 1 February 2009
Status: inactive
Page Count: 4
ICS Code (Solid wastes): 13.030.10
significance And Use:

A knowledge of the inorganic composition of a waste is often required for the selection of appropriate waste disposal practices. Solid waste may exist in a variety of forms and contain a range of... View More

scope:

1.1 This practice describes the digestion of solid waste using nitric acid for the subsequent determination of inorganic constituents by plasma emission spectroscopy or atomic absorption spectroscopy.

1.2 The following elements may be solubilized by this practice:

aluminummanganese
berylliummercury
cadmiumnickel
chromiumphosphorus
coppervanadium
ironzinc
lead

1.3 This practice is to be used when the concentrations of total recoverable elements are to be determined from a waste sample. Total recoverable elements may or may not be equivalent to total elements, depending on the element sought and the sample matrix. Recovery from refractory sample matrices, such as soils, is usually significantly less than total concentrations of the elements present.

Note 1-This practice has been used successfully for oily sludges and a municipal digested sludge standard [Environmental Protection Agency (EPA) Sample No. 397]. The practice may be applicable to some elements not listed above, such as arsenic, barium, selenium, cobalt, magnesium, and calcium. Refractory elements such as silicon, silver, and titanium, as well as organo-mercury are not solubilized by this practice.

1.4 This practice has been divided into two methods, A and B, to account for the advent of digestion blocks. Method A utilizes an electric hot plate; Method B utilizes an electric digestion block.

1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 7.

Document History

December 1, 2017
Standard Practice for Nitric Acid Digestion of Solid Waste
1.1 This practice describes the partial digestion of solid waste using nitric acid for the subsequent determination of the total recoverable content of inorganic constituents. 1.2 This practice is...
ASTM D5198-09
February 1, 2009
Standard Practice for Nitric Acid Digestion of Solid Waste
1.1 This practice describes the digestion of solid waste using nitric acid for the subsequent determination of inorganic constituents by plasma emission spectroscopy or atomic absorption...
April 10, 2003
Standard Practice for Nitric Acid Digestion of Solid Waste
1.1 This practice describes the digestion of solid waste using nitric acid for the subsequent determination of inorganic constituents by argon plasma emission spectroscopy or atomic absorption...
January 1, 1997
Standard Practice for Nitric Acid Digestion of Solid Waste
1.1 This practice describes the digestion of solid waste using nitric acid for the subsequent determination of inorganic constituents by argon plasma emission spectroscopy or atomic absorption...
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