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ASTM International - ASTM D7574-09

Standard Test Method for Determination of Bisphenol A in Environmental Waters by Liquid Chromatography/Tandem Mass Spectrometry

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Organization: ASTM International
Publication Date: 1 October 2009
Status: inactive
Page Count: 9
ICS Code (Examination of water for chemical substances): 13.060.50
significance And Use:

The first reported synthesis of BPA was by the reaction of phenol with acetone by Zincke. BPA has become an important high volume industrial chemical used in the manufacture of polycarbonate... View More

scope:

1.1 This procedure covers the determination of bisphenol A (BPA) extracted from water utilizing solid phase extraction (SPE), separated using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). BPA is qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 The method detection limit (MDL) and reporting limit (RL) for BPA are listed in Table 1.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

TABLE 1 MDL and Reporting Range

AnalyteMDL

A (ng/L)

Reporting Range

B (ng/L)

Bisphenol A520-600

A MDL determined following the Code of Federal Regulations, 40CFR Part 136, Appendix B.

B Lowest point of the reporting range, reporting limit, is calculated from the LV 1 concentration calibration standard in Table 4. Fig. 1 displays the signal/noise ratio at the reporting limit.

Document History

April 15, 2023
Standard Test Method for Determination of Bisphenol A in Environmental Waters by Liquid Chromatography/Tandem Mass Spectrometry
1.1 This test method covers the determination of bisphenol A (BPA) extracted from water utilizing solid phase extraction (SPE), separated using liquid chromatography (LC) and detected with tandem...
February 1, 2016
Standard Test Method for Determination of Bisphenol A in Environmental Waters by Liquid Chromatography/Tandem Mass Spectrometry
1.1 This procedure covers the determination of bisphenol A (BPA) extracted from water utilizing solid phase extraction (SPE), separated using liquid chromatography (LC) and detected with tandem mass...
ASTM D7574-09
October 1, 2009
Standard Test Method for Determination of Bisphenol A in Environmental Waters by Liquid Chromatography/Tandem Mass Spectrometry
1.1 This procedure covers the determination of bisphenol A (BPA) extracted from water utilizing solid phase extraction (SPE), separated using liquid chromatography (LC) and detected with tandem mass...
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