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ASTM International - ASTM E2890-12e1

Standard Test Method for Kinetic Parameters for Thermally Unstable Materials by Differential Scanning Calorimetry Using the Kissinger Method

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Organization: ASTM International
Publication Date: 1 September 2012
Status: inactive
Page Count: 11
ICS Code (Heat. Calorimetry): 17.200.10
significance And Use:

6.1 This test method is useful for research and development, quality assurance, regulatory compliance and specification-based acceptance.

6.2 The kinetic parameters determined by this... View More

scope:

1.1 This test method describes the determination of the kinetic parameters of Arrhenius activation energy and pre-exponential factor using the Kissinger variable heating rate iso-conversion method (1, 2)2 and activation energy and reaction order by the Farjas method (3) for thermally unstable materials. The test method is applicable to the temperature range from 300 to 900 K (27 to 627°C).

1.2 Both nth order and accelerating reactions are addressed by this method over the range of 0.5 < n < 4 and 1 < p < 4 where n is the nth order reaction order and p is the Avrami reaction order (4). Reaction orders n and p are determined by the Farjas method (3).

1.3 This test method uses the same experimental conditions as Test Method E698. The Flynn/Wall/Ozawa data treatment of Test Method E698 may be simultaneously applied to these experimental results.

1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5 There is no ISO equivalent to this standard.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Document History

April 1, 2018
Standard Test Method for Kinetic Parameters for Thermally Unstable Materials by Differential Scanning Calorimetry Using the Kissinger Method
1.1 This test method describes the determination of the kinetic parameters of Arrhenius activation energy and pre-exponential factor using the Kissinger variable heating rate iso-conversion method...
September 1, 2012
Standard Test Method for Kinetic Parameters for Thermally Unstable Materials by Differential Scanning Calorimetry Using the Kissinger Method
1.1 This test method describes the determination of the kinetic parameters of Arrhenius activation energy and pre-exponential factor using the Kissinger variable heating rate iso-conversion method...
ASTM E2890-12e1
September 1, 2012
Standard Test Method for Kinetic Parameters for Thermally Unstable Materials by Differential Scanning Calorimetry Using the Kissinger Method
1.1 This test method describes the determination of the kinetic parameters of Arrhenius activation energy and pre-exponential factor using the Kissinger variable heating rate iso-conversion method...
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