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ASTM International - ASTM D7035-16

Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)

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Organization: ASTM International
Publication Date: 1 October 2016
Status: active
Page Count: 29
ICS Code (Ambient atmospheres): 13.040.20
significance And Use:

5.1 The health of workers in many industries is at risk through exposure by inhalation to toxic metals and metalloids. Industrial hygienists and other public health professionals need to determine... View More

scope:

1.1 This test method specifies a procedure for collection, sample preparation, and analysis of airborne particulate matter for the content of metals and metalloids using inductively coupled plasma-atomic emission spectrometry (ICP-AES).

1.2 This test method is applicable to personal sampling of the inhalable or respirable fraction of airborne particles and to area sampling.

1.3 This test method should be used by analysts experienced in the use of ICP-AES, the interpretation of spectral and matrix interferences, and procedures for their correction.

1.4 This test method specifies a number of alternative methods for preparing test solutions from samples of airborne particulate matter. One of the specified sample preparation methods is applicable to the measurement of soluble metal or metalloid compounds. Other specified methods are applicable to the measurement of total metals and metalloids.

1.5 It is the user's responsibility to ensure the validity of this test method for sampling materials of untested matrices.

1.6 The following is a non-exclusive list of metals and metalloids for which one or more of the sample dissolution methods specified in this document is applicable. However, there is insufficient information available on the effectiveness of dissolution methods for those elements in italics.

Aluminum

Indium

Sodium
Antimony Iron Strontium
Arsenic Lead

Tantalum

Barium Lithium Tellurium
Beryllium Magnesium Thallium
Bismuth Manganese Tin
Boron Molybdenum Titanium
Cadmium Nickel Tungsten
Calcium Phosphorus

Uranium

Cesium Platinum Vanadium
Chromium Potassium Yttrium
Cobalt

Rhodium

Zinc
Copper Selenium Zirconium

Hafnium

Silver  

1.7 This test method is not applicable to the sampling of elemental mercury, or to inorganic compounds of metals and metalloids that are present in the gaseous or vapor state.

1.8 No detailed operating instructions are provided because of differences among various makes and models of suitable ICP-AES instruments. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular instrument. This test method does not address comparative accuracy of different devices or the precision between instruments of the same make and model.

1.9 This test method contains notes that are explanatory and are not part of the mandatory requirements of this test method.

1.10 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.11 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Document History

ASTM D7035-16
October 1, 2016
Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
1.1 This test method specifies a procedure for collection, sample preparation, and analysis of airborne particulate matter for the content of metals and metalloids using inductively coupled...
April 1, 2010
Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
1.1 This test method specifies a procedure for collection, sample preparation, and analysis of airborne particulate matter for the content of metals and metalloids using inductively coupled...
October 1, 2004
Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
1.1 This test method specifies a procedure for collection, sample preparation, and analysis of airborne particulate matter for the content of metals and metalloids using inductively coupled...
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