Standard Practice for Separation and Concentration of Ignitable Liquid Residues from Fire Debris Samples by Passive Headspace Concentration with Solid Phase Microextraction (SPME)
|Publication Date:||10 September 2001|
|ICS Code (Liquid and solid fuel burners):||27.060.10|
This practice describes the procedure for removing small quantities of ignitable liquid residues from samples of fire debris. An adsorbent material is used to extract the residue from the static headspace above the sample. Then, analytes are thermally desorbed in the injection port of the gas chromatograph (GC).
This practice is best suited for screening fire debris samples to assess relative ignitable liquid concentration and for extracting ignitable liquid from aqueous samples.
This practice is suitable for extracting ignitable liquid residues when a high level of sensitivity is required due to a very low concentration of ignitable liquid residues in the sample.
Unlike other methods of separation and concentration, this method recovers a minimal amount of the ignitable residues present in the evidence, leaving residues that are suitable for subsequent resampling.
Alternate separation and concentration procedures are listed in Section 2.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.