UNLIMITED FREE ACCESS TO THE WORLD'S BEST IDEAS

SUBMIT
Already an Engineering360 user? Log in.

This is embarrasing...

An error occurred while processing the form. Please try again in a few minutes.

Customize Your Engineering360 Experience

Finish!
Privacy Policy

This is embarrasing...

An error occurred while processing the form. Please try again in a few minutes.

ASTM International - ASTM D5394-02(2012)

Standard Specification for Reclaimed 1,1,1-Trichloroethane (Withdrawn 2017)

inactive
Buy Now
Organization: ASTM International
Publication Date: 1 March 2012
Status: inactive
Page Count: 2
ICS Code (Halogenated hydrocarbons): 71.080.20
scope:

1.1 This specification defines Type I (high quality reclaimed 1,1,1-trichloroethane, approximating MIL Specification), Type II (good quality reclaimed solvent), Type III (minimal acceptable reclaimed solvent).

1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific hazards statement see Section 4.

1.3 1,1,1-trichloroethane also is known commercially as methyl chloroform.

TABLE 1 Properties, Type I

PropertySpecificationTest Method
AppearanceFree of turbidity and suspended matter

D3741

1,1,1-trichloroethane, weight %,
min
92

D6806

Nonvolatile residue, weight
%, max
0.0040

D2109

Color, Pt-Co, max25

D2108

Water, weight %, max0.015

D3401

Acid acceptance as NaOH, weight
%, min
0.20

D2942

Aluminum scratch testPasses

A

D2943

Acidity as HCl, weight %, max0.001

D2989

Alkalinity as NaOH, weight %, max0.020

D2106

Halide as Cl, weight %, max0.0005

D2988

A Distill 100 mL solvent, collect 50 mL distillate, and conduct scratch test on distillate and portion remaining in distillation flask.

TABLE 2 Properties, Type II

PropertySpecificationTest Method
AppearanceFree of turbidity and
suspended matter

D3741

1,1,1-trichloroethane, weight %,
min
90

D6806

Nonvolatile residue (NVR), weight
%, max
0.010

D2109

Color, Pt-Co, max30

D2108

Water, weight %, max0.015

D3401

Acid acceptance as NaOH, weight
%, min
0.20

D2942

Aluminum scratch testPasses

A

D2943

Acidity as HCl, weight %, max0.001

D2989

Alkalinity as NaOH, weight %, max0.020

D2106

Halide as Cl, weight %, max0.0005

D2988

A Distill 100 mL solvent, collect 50 mL distillate, and conduct scratch test on distillate and portion remaining in distillation flask.

TABLE 3 Properties, Type IIIA

PropertySpecificationTest Method
AppearanceFree of turbidity and
suspended matter

D3741

1,1,1-trichloroethane, weight %,
min
88

D6806

Nonvolatile residue, weight
%, max
0.020

D2109

Color, Pt-Co, max50

D2108

Water, weight %, max0.020

D3401

Acid acceptance as NaOH, weight
%, min
0.20

D2942

Aluminum scratch testPasses

B

D2943

Acidity as HCl, weight %, max0.002

D2989

Alkalinity as NaOH, weight %, max0.020

D2106

A Type III reclaimed 1,1,1-trichloroethane is not recommended for use in precision cleaning or vapor degreasing applications.

B Distill 100 mL solvent, collect 50 mL distillate, and conduct scratch test on distillate and portion remaining in distillation flask.

abstract:

This specification defines reclaimed 1,1,1-trichloroethane, also known commercially as methyl chloroform. The types are defined: Type I - high quality reclaimed 1,1,1-trichloroethanView More

Document History

ASTM D5394-02(2012)
March 1, 2012
Standard Specification for Reclaimed 1,1,1-Trichloroethane (Withdrawn 2017)
1.1 This specification defines Type I (high quality reclaimed 1,1,1-trichloroethane, approximating MIL Specification), Type II (good quality reclaimed solvent), Type III (minimal acceptable reclaimed...
February 1, 2007
Standard Specification for Reclaimed 1,1,1-Trichloroethane
1.1 This specification defines Type I (high quality reclaimed 1,1,1-trichloroethane, approximating MIL Specification), Type II (good quality reclaimed solvent), Type III (minimal acceptable reclaimed...
December 10, 2002
Standard Specification for Reclaimed 1,1,1-Trichloroethane
1.1 This specification defines Type I (high quality reclaimed 1,1,1-trichloroethane, approximating MIL Specification), Type II (good quality reclaimed solvent), Type III (minimal acceptable reclaimed...
May 10, 1997
Standard Specification for Reclaimed 1,1,1-Trichloroethane
1.1 This specification defines Type I (high quality reclaimed 1,1,1-trichloroethane, approximating MIL Specification), Type II (good quality reclaimed solvent), Type III (minimal acceptable reclaimed...
Advertisement